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Detection of Storage Age Adulteration in Khao Dawk Mali 105 Rice using Near-Infrared Spectroscopy

Detection of Storage Age Adulteration in Khao Dawk Mali 105 Rice  using Near-Infrared Spectroscopy

Abstract

This research aims to investigate the adulteration of Khao Dawk Mali 105 rice based on storage age using Near-Infrared Spectroscopy (NIRS) with Fourier Transform Near-Infrared Spectroscopy (FT-NIR) in the wavenumber range of 12,500 – 4,000 cm-1 (800 – 2,500 nm). Storage duration significantly impacts the quality of cooked rice. This research is divided into two parts: 1) to investigate the feasibility of separating rice according to storage age (1, 2, and 3 years) using the best model created by an Ensemble method combined with Second Derivative, which achieved an accuracy of 96.3%. 2) To investigate adulteration based on storage age by adulterating at 0% (all 2- and 3-year-old rice), 10%, 20%, 30%, 40%, 50%, 60%, 70%, 80%, 90%, and 100% (all 1-year-old rice). The best model was created using Gaussian Process Regression (GPR) combined with Smoothing + Multiplicative Scatter Correction (MSC), with coefficients of determination (r²), root mean square error of prediction (RMSEP), bias, and prediction ability (RPD) values of 0.92, 8.6%, 0.9%, and 3.6 respectively. This demonstrates that the adulteration model can be applied to separate rice by storage age (1, 2, and 3 years). Additionally, the color values of rice with different storage ages show differences in L* and b* values.

Objective

โรงงานผู้ผลิตข้าวพบปัญหาการปลอมปนของข้าวสารที่มีอายุการเก็บรักษาต่างกัน โดยทั่วไปการคัดแยกการปลอมปนจะใช้วิธีมาตรฐานโดยการหุงข้าว จากนั้นนำข้าวหุงสุกไปวัดเนื้อสัมผัสเพื่อแยกอายุของข้าว ซึ่งใช้เวลาและเป็นการทำลายตัวอย่างและเกิดความล่าช้าในการตรวจสอบคุณภาพข้าวสาร งานวิจัยนี้ใช้เทคนิคเนียร์อินฟราเรดสเปกโทรสโกปี (Near-Infrared Spectroscopy, NIRS) ในการตรวจสอบการปลอมปนของข้าวสารพันธุ์ขาวดอกมะลิ 105 (KDML 105) ที่อายุการเก็บรักษาต่างกันเพื่อแก้ไขปัญหาดังกล่าว

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